Laboratory & Lecture Schedule

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Master Laboratory/Lecture Schedule
Chemistry 3152, Fall 2007
Professors Mark C. Morvant and Kenneth M. Nicholas and Teaching Assistants

Week		Monday		Tuesday		Wednesday		Thursday		Tues Lecture**
Aug.	20	Check-in/	21	Check-in/	22	Exp. 1	23	Exp. 1	21	Live Lecture
1		Intro. 0		Intro. 0		Simple Distillation		Simple Distillation		Introduction
Aug.	27	Exp. 2	28	Exp. 2	29	Exp. 2	30	Exp. 2	28	Live/Streamed
2		Fractional Distillation		Fractional Distillation		Fractional Distillation		Fractional Distillation		Distillation/ Chromatography
Sept.	3		4		5	Exp. 3	6	Exp. 3	4	Live/Streamed
3		NO LAB		NO LAB		Isomerization		Isomerization		Extraction/ Natural Products
Sept.	10		11		12		13		11	Live/Streamed
4		Ext. of Nutmeg		Ext. of Nutmeg		Fermentation/ Distillation		Fermentation/ Distillation		Partitioning/ Sublimation
Sept.	17	Exp. 4	18	Exp. 4	19	Exp. 5	20	Exp. 5	18	Live/Streamed
5		Partition Coefficient		Partition Coefficient		Isolation of Caffeine		Isolation of Caffeine		Diels-Alder/ Friedel-Crafts
Sept.	24	Exp. 5	25	Exp. 5	26	Exp. 6	27	Exp. 6	25	Live/Streamed
6		Isolation of Caffeine		Isolation of Caffeine		Diels-Alder Reaction		Diels-Alder Reaction		Chromatography
October	1	Exp. 7	2	Exp. 7	3	Exp. 7	4	Exp. 7	2	Live/Streamed
7		Friedel-Crafts Acetylation		Friedel-Crafts Acetylation		Friedel-Crafts Acetylation		Friedel-Crafts Acetylation		Oxidation/ Reduction
October	8	Exp. 7	9	Exp. 7	10	Exp. 8	11	Exp. 8	9	Live Lecture
8		Friedel-Crafts Acetylation		Friedel-Crafts Acetylation		Hydrobor.-Oxidation		Hydrobor.-Oxidation		Review
October	15	Exp. 8	16	Exp. 8	17	Exp. 9	18	Exp. 9	16
9		Hydrobor.-Oxidation		Hydrobor.-Oxidation		Chromium Oxidation		Chromium Oxidation		Mid-Term Exam
October	22	Exp. 10	23	Exp. 10	24	Exp. 11	25	Exp. 11	23	Live/Streamed
10		Williamson Synthesis		Williamson Synthesis		NaBH4 Reduction		NaBH4 Reduction		IR
October	29	Exp. 13	30	Exp. 13	31	Exp. 13	1	Exp. 13	29	Live/Streamed
11		Grignard Reaction		Grignard Reaction		Grignard Reaction		Grignard Reaction		NMR
Nov.	5	Exp. 14a	6	Exp. 14a	7	Exp. 14b	8	Exp. 14b	6	Live/Streamed
12		Multi-step		Multi-step		Multi-step		Multi-step		NMR
Nov.	12	Exp. 14c	13	Exp. 14c	14	Exp. 14d	15	Exp. 14d	13	Live/Streamed
13		Multi-step		Multi-step		Multi-step		Multi-step		IR/NMR
Nov.	19	Exp. 15	20	Exp. 15	21		22		20	Live/Streamed
14		Wittig Reaction		Wittig Reaction		NO LAB		NO LAB		Spectroscopy Review
Nov.	26	Exp. 15	27	Exp. 15	28	Exp. 17	29	Exp. 17	27	Live Lecture
15		Wittig Reaction		Wittig Reaction		Acetanilide		Acetanilide		Review
Dec.	3		4		5		6		4
16		Check- out		Check- out						Final Exam

**Much of the information you will need for laboratory preparation will be given in streamed lectures.  You are completely responsible for all information in the streamed lectures.  Several of the Tuesday lecture periods will be used for review and problem solving as indicated here.